Kozechko V. Formation of a complex of mechanical properties of lowcarbon microalloyed steels depending on the thickness of the rolled metal

Українська версія

Thesis for the degree of Doctor of Philosophy (PhD)

State registration number

0824U003598

Applicant for

Specialization

  • 132 - Матеріалознавство

17-12-2024

Specialized Academic Board

ДФ 08.080.067

Dnipro University of Technology

Essay

Thick plates have a wide range of applications. They can form both crosssections of load-bearing structural elements and dense, strong shells used for the storage, handling, transportation, and processing of liquids, gases, and bulk materials. In construction, thick plate rolled metal is primarily used in the production of welded structural frames for buildings and structures. It is worth noting that the current regulatory documentation requires the use of rolled metal of uniform thickness across the cross-section of structural elements in the design of welded metal structures. However, an analysis of the distribution of external loads across the cross-section of structures shows that in some cases, plates of varying thickness should be used in the production of structures. Low-carbon microalloyed steel 10G2FB was selected as the material for the study, with thicknesses of 16, 20, 30, 40, 50, 70, and 100 mm. In accordance with the set objective, the study investigated properties that characterize the kinetics of material failure, specifically the material's ability to resist crack initiation and propagation. The experimental methods included static mechanical testing (tensile testing) and dynamic mechanical testing (impact bending testing). The study of the morphology of structural components and fracture surfaces was conducted in stages: 1. First Stage: Examination of samples at low magnification (metallographic analysis). 2. Second Stage: Examination of samples at medium and relatively high magnification (scanning electron microscopy). 3. Third Stage: Examination of fracture surfaces (scanning electron microscopy). Microstructural analysis revealed that the microstructural components of all studied systems are ferrite and pearlite. The 16 mm thick steel exhibits a ferrite-pearlite structure in a 70%-30% ratio, respectively. As the thickness increases, the percentage of ferrite increases while the percentage of pearlite decreases. For the 100 mm thick steel, the microstructure consists of 80% ferrite and 20% pearlite. Ferrite forms as grains with a polyhedral shape, while pearlite colonies are located in segregation bands. Analysis of the fine structure showed that for all thicknesses of rolled metal, the grains of the ferritic phase have a regular polyhedral shape. Nucleation of new phases most frequently occurs on the surface of austenite grains and inclusions. Subsequently, cementite and ferrite grow gradually as roughly equiaxed formations. At a certain point, cementite nuclei form along grain boundaries and grow as plates into the grain interior. This process results in alternating recrystallization of cementite and ferrite, which propagates along the boundaries. Pearlite colonies appear and continue to grow until they come into contact with each other. The dissertation demonstrates that as the thickness of the rolled metal increases, there is a change in the shape of the cementite framework within pearlite colonies from spherical to fan-like. This phenomenon is explained by corresponding changes in cooling conditions with increasing thickness. Based on the quantitative data obtained on the dependence of the percentage of structural components on the thickness of the rolled metal, regression models were developed. Analysis of these models shows that the observed dependencies are nonlinear and can be described by logarithmic equations of the form Y = b0 + b1хlog10(x). Fractographic analysis of fracture surfaces revealed that for the 16 mm thickness, fracture occurs due to shear failure, characterized by smooth surfaces and steps—signs indicative of a quasi-cleavage mechanism. According to metallographic analysis, the structure of the rolled metal of this thickness contains ferrite and pearlite. Therefore, it can be assumed that the brittle fracture characteristics are associated with pearlite colonies. At the initial stage of facet formation, quasi-cleavage shows signs of predominantly crystalline separation, while in areas of microcrack coalescence, signs of ductile fracture are observed.

Research papers

Beketov, O., Laukhin, D., Rott, N., Babenko, E., Kozechko, V. (2024). Use of the Processing Arrays Theory of Experimental Data for the Analysis of the Technological Scheme in the Rolled Metal Production – Controlled Rolling. In: Ivanov, V., Trojanowska, J., Pavlenko, I., Rauch, E., Piteľ, J. (eds) Advances in Design, Simulation and Manufacturing VII. DSMIE 2024. Lecture Notes in Mechanical Engineering. Springer, Cham.

Лаухін, Д. В., Бекетов, О. В., Дадіверіна, Л. М., & Козечко, В. І. (2023). Дослідження взаємозв’язку між температурою кінця гарячої деформації та комплексом механічних властивостей низьковуглецевих сталей на основі аналізу регресійних моделей // Математичне моделювання, (2 (49)), 182-197.

Дослідження взаємозв’язку між товщиною та структурним станом металопрокату з низьковуглецевої низьколегованої сталі10Г2ФБ / О. В. Бекетов, Д. В. Лаухін, Л. М. Дадіверіна та ін. // Український журнал будівництва та архітектури. – 2024. – № 2. – С. 26-33

Козечко В.І. Особливості виробництва зварних труб великого діаметру та спосіб їх термічної обробки // Збірник наукових праць НГУ, №68-14, Дніпро, 2022, с. 157-165

Козечко В. А. Особливості зміни мікроструктури і механічних характеристик при високоенергетичному навантаженні / В. А. Козечко, В. І. Козечко. // Збірник наукових праць НГУ. – 2023. – №74-1. – С. 154–162.

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